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N-(2-Methoxyphenyl)acetamide

$64

  • Brand : BIOFRON

  • Catalogue Number : BN-O1037

  • Specification : 98%(HPLC)

  • CAS number : 93-26-5

  • Formula : C9H11NO2

  • Molecular Weight : 165.19

  • PUBCHEM ID : 7135

  • Volume : 5mg

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Catalogue Number

BN-O1037

Analysis Method

Specification

98%(HPLC)

Storage

2-8°C

Molecular Weight

165.19

Appearance

Botanical Source

Structure Type

Category

SMILES

CC(=O)NC1=CC=CC=C1OC

Synonyms

Ethanimidic acid, N-(2-methoxyphenyl)-, (1E)-/N-(2-Methoxyphenyl)acetamide/2'-Methoxyacetanilide/(1E)-N-(2-Methoxyphenyl)ethanimidic acid/Acetamide, N- (2-methoxyphenyl)-/N-(2-Methoxy-phenyl)-acetamide/Acetamide, N-(2-methoxyphenyl)-

IUPAC Name

N-(2-methoxyphenyl)acetamide

Density

1.1±0.1 g/cm3

Solubility

Flash Point

146.2±28.4 °C

Boiling Point

318.2±44.0 °C at 760 mmHg

Melting Point

70-74 °C(lit.)

InChl

InChI=1S/C22H20N2O5/c1-3-11-5-6-17(25)13-7-12-9-24-16(19(12)23-18(11)13)8-15-14(20(24)26)10-29-21(27)22(15,28)4-2/h5-8,25,28H,3-4,9-10H2,1-2H3/t22-/m0/s1

InChl Key

FGOFNVXHDGQVBG-UHFFFAOYSA-N

WGK Germany

RID/ADR

HS Code Reference

Personal Projective Equipment

Correct Usage

For Reference Standard and R&D, Not for Human Use Directly.

Meta Tag

provides coniferyl ferulate(CAS#:93-26-5) MSDS, density, melting point, boiling point, structure, formula, molecular weight etc. Articles of coniferyl ferulate are included as well.>> amp version: coniferyl ferulate

No Technical Documents Available For This Product.

PMID

30736295

Abstract

Three new complexes [Mo(η3-C3H5)Br(CO)2{iPrN=C(R)C5H4N}], where R = H (IMP = N-isopropyl 2-iminomethylpyridine), Me, and Ph, were synthesized and characterized, and were fluxional in solution. The most interesting feature was the presence, in the crystal structure of the IMP derivative, of the two main isomers (allyl and carbonyls exo), namely the equatorial isomer with the Br trans to the allyl and the equatorial with the Br trans to one carbonyl, the position trans to the allyl being occupied by the imine nitrogen atom. For the R = Me complex, the less common axial isomer was observed in the crystal. These complexes were immobilized in MCM-41 (MCM), following functionalization of the diimine ligands with Si(OEt)3, in order to study the catalytic activity in olefin epoxidation of similar complexes as homogeneous and heterogeneous catalysts. FTIR, 13C- and 29Si-NMR, elemental analysis, and adsorption isotherms showed that the complexes were covalently bound to the MCM walls. The epoxidation activity was very good in both catalysts for the cis-cyclooctene and cis-hex-3-en-1-ol, but modest for the other substrates tested, and no relevant differences were found between the complexes and the Mo-containing materials as catalysts.

KEYWORDS

molybdenum, allyl complexes, isomers, crystal structures, iminomethylpyridine, epoxidation

Title

New Molybdenum(II) Complexes with α-Diimine Ligands: Synthesis, Structure, and Catalytic Activity in Olefin Epoxidation

Author

Maria Vasconcellos-Dias,1 João Marreiros,1 Rita Sales,1 Vitor Felix,2 Paula Brandão,2 Carla D. Nunes,1,3 and Maria Jose Calhorda1,4,*

Publish date

2019 Feb;

PMID

29304126

Abstract

Objective
To develop a Chinese version of the Newest Vital Sign (NVS-CHN) instrument and evaluate its psychometric properties.

Methods
To deal with cross-cultural adaptation problems, after translation of the NVS into Chinese, the Delphi method was used for experts and cognitive testing was used for participants. A cross-sectional study including 351 participants was conducted to assess the validity of the NVS-CHN. Internal reliability, criterion validity, and known-groups validity were investigated. The NVS-CHN was further validated against a suitable standard, the Chinese Citizen Health Literacy Questionnaire (CCHLQ).

Results
The validity of the NVS-CHN was established by conducting a Delphi survey (three rounds) and cognitive testing (three rounds). Cronbach’s alpha was 0.71, indicating that internal consistency was acceptable. A Spearman’s correlation coefficient of 0.68 between the NVS-CHN and CCHLQ revealed excellent criterion validity. Differences in NVS-CHN scores by education level confirmed known-groups validity. A receiver operating characteristics analysis showed that the area under the curve was 0.81, indicating that the NVS-CHN was an accurate health literacy assessment tool. A score ≥ 4 out of 6 best identified participants with adequate health literacy.

Conclusions
The NVS-CHN has excellent psychometrical reliability and validity, which make it a suitable tool to evaluate health literacy in China.

Title

Validation of a newly adapted Chinese version of the Newest Vital Sign instrument

Author

Jin Xue, Investigation, Validation, Writing - original draft,#1,2 Yongbing Liu, Conceptualization, Supervision, Validation, Writing - review & editing,#3 Kaixuan Sun, Conceptualization, Formal analysis, Validation,1,3 Linfeng Wu, Investigation, Validation,1,3 Kai Liao, Resources,1 Yan Xia, Formal analysis,3 Ping Hou, Conceptualization, Investigation,3 Huiping Xue, Investigation,3 and Hongcan Shi, Data curation, Funding acquisition, Writing - review & editing1,*

Publish date

2018;

PMID

21173724

Abstract

During our screening program for agrochemicals from Chinese medicinal herbs and wild plants, the essential oil of Carum carvi fruits was found to possess strong contact toxicity against Sitophilus zeamais and Tribolium castaneum adults, with LD50 values of 3.07 and 3.29 μg/adult, respectively, and also showed strong fumigant toxicity against the two grain storage insects with LC50 values of 3.37 and 2.53 mg/L, respectively. The essential oil obtained by hydrodistillation was investigated by GC and GC-MS. The main components of the essential oil were identified to be (R)-carvone (37.98%) and D-limonene (26.55%) followed by α-pinene (5.21), cis-carveol (5.01%) and β-myrcene (4.67%). (R)-Carvone and D-limonene were separated and purified by silica gel column chromatography and preparative thin layer chromatography, and further identified by means of physicochemical and spectrometric analysis. (R)-Carvone and D-limonene showed strong contact toxicity against S. zeamais (LD50 = 2.79 and 29.86 μg/adult) and T. castaneum (LD50 = 2.64 and 20.14 μg/adult). (R)-Carvone and D-limonene also possessed strong fumigant toxicity against S. zeamais (LC50= 2.76 and 48.18 mg/L) and T. castaneum adults (LC50= 1.96 and 19.10 mg/L).

KEYWORDS

Carum carvi, Sitophilus zeamais, Tribolium castaneum, fumigant, contact toxicity, essential oil, (R)-carvone, D-limonene

Title

Insecticidal Activity of Essential Oil of Carum Carvi Fruits from China and Its Main Components against Two Grain Storage Insects

Author

Rui Fang,1 Cai Hong Jiang,2 Xiu Yi Wang,3 Hai Ming Zhang,1 Zhi Long Liu,2,* Ligang Zhou,4 Shu Shan Du,1,* and Zhi Wei Deng3

Publish date

2010 Dec


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